In situ analysis of the degree of polymerization of bone cement by using FT-Raman spectroscopy

Rehman, I. and Harper, E.J. and Bonfield, W. (1996) In situ analysis of the degree of polymerization of bone cement by using FT-Raman spectroscopy. Biomaterials, 17 (16). pp. 1615-1619. ISSN 0142-9612

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Abstract

A method has been developed which enables an in situ analysis of the degree of polymerization of bone cement. The concentration of monomeric double bond is monitored continuously during the entire curing process and hence the method can be used for quantitative studies of polymerization kinetics. In this study, Fourier Transform Raman (FTR) spectroscopy was utilized to investigate the degree of polymerization of a novel bone cement in situ, and the results are compared with the thermal profile obtained for polymerization. A method has been developed which enables an in situ analysis of the degree of polymerization of bone cement. The concentration of monomeric double bond is monitored continuously during the entire curing process and hence the method can be used for quantitative studies of polymerization kinetics. In this study, Fourier Transform Raman (FTR) spectroscopy was utilized to investigate the degree of polymerization of a novel bone cement in situ, and the results are compared with the thermal profile obtained for polymerization.

Item Type:
Journal Article
Journal or Publication Title:
Biomaterials
Uncontrolled Keywords:
/dk/atira/pure/subjectarea/asjc/2500/2502
Subjects:
?? bone cementft-raman spectroscopyin situ analysisthermal profilesaddition reactionschemical bondscuringin situ processingmedical applicationspolymerizationraman spectroscopyfourier transform raman spectroscopybone cementarticlefourier transformationpolymer ??
ID Code:
132888
Deposited By:
Deposited On:
16 Apr 2019 13:25
Refereed?:
Yes
Published?:
Published
Last Modified:
15 Jul 2024 19:17