A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite

Laurencin, Danielle and Wong, Alan and Hanna, John V. and Dupree, Ray and Smith, Mark E. (2008) A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite. Journal of the American Chemical Society, 130 (8). pp. 2412-2413. ISSN 1520-5126

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Abstract

High resolution Ca-43 solid-state NMR studies of hydroxyapatite (Ca-10(PO4)(6)(OH2)) were performed at 14.1 T. The two crystallographically distinct calcium sites were unequivocally resolved by a triple-quantum magic angle spinning experiment, and the unambiguous assignment of the signals was possible using H-1-Ca-43 rotational echo double resonance and H-1-Ca-43 cross polarization magic angle spinning experiments.

Item Type:
Journal Article
Journal or Publication Title:
Journal of the American Chemical Society
Uncontrolled Keywords:
/dk/atira/pure/subjectarea/asjc/1500/1503
Subjects:
Departments:
ID Code:
52857
Deposited By:
Deposited On:
29 Feb 2012 09:38
Refereed?:
Yes
Published?:
Published
Last Modified:
13 May 2020 01:45