Effect of Poly-γ-Glutamic Acid Molecular Weight on the Properties of Whey Protein Isolate Hydrogels

Baines, Daniel K. and Pawlak-Likus, Zuzanna and Tavernaraki, Nikoleta N. and Platania, Varvara and Parati, Mattia and Cheung, Timothy N. Wong Wong and Radecka, Iza and Domalik-Pyzik, Patrycja and Chatzinikolaidou, Maria and Douglas, Timothy E. L. (2025) Effect of Poly-γ-Glutamic Acid Molecular Weight on the Properties of Whey Protein Isolate Hydrogels. Polymers, 17 (12): 1605. ISSN 2073-4360

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Abstract

Whey protein isolate (WPI) hydrogel is a promising candidate as a biomaterial for tissue engineering. Previously, WPI hydrogels containing poly-γ-glutamic acid (γ-PGA) with a molecular weight (MW) of 440 kDa demonstrated potential as scaffolds for bone tissue engineering. Here, the study compares different γ-PGA preparations of differing MW. WPI-γ-PGA hydrogels containing 40% WPI and 0%, 2.5%, 5%, 7.5%, and 10% γ-PGA were synthesised. Three γ-PGA MWs were compared, namely 10 kDa, 700 kDa, and 1100 kDa. Evidence of successful γ-PGA incorporation was demonstrated by scanning electron microscopy and Fourier transform infrared spectroscopy. Increasing γ-PGA concentration significantly improved the swelling potential of the hydrogels, as demonstrated by ratio mass increases of between 85 and 90% for each 10% variable group. Results suggested that γ-PGA delayed enzymatic proteolysis, potentially decreasing the rate of degradation. The addition of γ-PGA significantly decreased the Young’s modulus and compressive strength of hydrogels. Dental pulp mesenchymal stem cells proliferated on all hydrogels. The highest cellular growth was observed for the WPI-700 kDa γ-PGA group. Additionally, superior cell attachment was observed on all WPI hydrogels containing γ-PGA compared to the WPI control. These results further suggest the potential of WPI hydrogels containing γ-PGA as biomaterials for bone tissue engineering.

Item Type:
Journal Article
Journal or Publication Title:
Polymers
Uncontrolled Keywords:
/dk/atira/pure/subjectarea/asjc/1600
Subjects:
?? chemistry(all)polymers and plastics ??
ID Code:
230169
Deposited By:
Deposited On:
20 Jun 2025 09:10
Refereed?:
Yes
Published?:
Published
Last Modified:
21 Jun 2025 02:40