Rapid synthesis of hydrogen bond templated handcuff rotaxanes

Barlow, Sean R. and Tomkinson, David and Halcovitch, Nathan R. and Evans, Nicholas H. (2024) Rapid synthesis of hydrogen bond templated handcuff rotaxanes. Organic and Biomolecular Chemistry. ISSN 1477-0520

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Abstract

The rapid synthesis of hydrogen bond templated handcuff rotaxanes is described. The isolated rotaxanes were characterized by NMR and IR spectroscopies and high resolution mass spectrometry. This report represents a rare demonstration of preparing (2)handcuff [2]rotaxanes by covalently linking separate axles threaded through the rings of a bis-macrocycle by use of the copper catalyzed azide-alkyne cycloaddition (CuAAC) reaction.

Item Type:
Journal Article
Journal or Publication Title:
Organic and Biomolecular Chemistry
Uncontrolled Keywords:
Research Output Funding/yes_externally_funded
Subjects:
?? yes - externally fundedyesbiochemistryorganic chemistryphysical and theoretical chemistry ??
ID Code:
221220
Deposited By:
Deposited On:
10 Jun 2024 10:05
Refereed?:
Yes
Published?:
Published
Last Modified:
18 Jun 2024 01:02