The synthesis and molecular structure of 1-(3,4-dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one hydrochloride methanol solvate

Hall, Steven R. and Roy, Raymond and McLaughlin, Dylan T. and Sullivan, Kate J. and Barclay, Ross C. and Vogels, Christopher M. and Decken, Andreas and Westcott, Stephen A. (2013) The synthesis and molecular structure of 1-(3,4-dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one hydrochloride methanol solvate. Crystals, 3 (2). pp. 333-338. ISSN 2073-4352

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Abstract

A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic space group P-1 with unit cell parameters a = 8.3801(11) Å; b = 9.2583(12) Å; c = 11.5671(15) Å; α = 73.566(2)°; β = 84.514(2)°; γ = 66.578(2)°. The asymmetric unit contains two molecules.

Item Type:
Journal Article
Journal or Publication Title:
Crystals
Uncontrolled Keywords:
/dk/atira/pure/subjectarea/asjc/1500/1500
Subjects:
?? dopaminehydroxypyridinoneligandx-raygeneral chemical engineeringgeneral materials sciencecondensed matter physicsinorganic chemistrymaterials science(all)chemical engineering(all) ??
ID Code:
214168
Deposited By:
Deposited On:
06 Feb 2024 09:40
Refereed?:
Yes
Published?:
Published
Last Modified:
04 Oct 2024 00:25