Reaction workup planning:A structured flowchart approach, exemplified in difficult aqueous workup of hydrophilic products

Hill, George B. and Sweeney, Joseph B. (2015) Reaction workup planning:A structured flowchart approach, exemplified in difficult aqueous workup of hydrophilic products. Journal of Chemical Education, 92 (3). pp. 488-496. ISSN 0021-9584

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Abstract

Reaction workup can be a complex problem for those facing novel synthesis of difficult compounds for the first time. Workup problem solving by systematic thinking should be inculcated as mid-graduate-level is reached. A structured approach is proposed, building decision tree flowcharts to analyze challenges, and an exemplar flowchart is presented for aqueous workup of awkwardly hydrophilic products. Its use is illustrated with real synthetic compounds and model examples.

Item Type:
Journal Article
Journal or Publication Title:
Journal of Chemical Education
Uncontrolled Keywords:
/dk/atira/pure/subjectarea/asjc/3300/3304
Subjects:
ID Code:
123725
Deposited By:
Deposited On:
26 Feb 2018 12:10
Refereed?:
Yes
Published?:
Published
Last Modified:
06 May 2020 05:42