Savin, Shelley L. P. and Chadwick, Alan V. and O'Dell, Luke A. and Smith, Mark E. (2007) Characterisation of nanocrystalline magnesium oxide by X-ray absorption spectroscopy. ChemPhysChem, 8 (6). pp. 882-889. ISSN 1439-7641
Full text not available from this repository.Official URL: http://dx.doi.org/10.1002/cphc.200600750
Abstract
27Al MAS NMR has been used to study a sol?gel prepared alumina annealed at various temperatures. Two-field simulation of the sample heated to 1200 ?C confirmed the presence of corundum, as suggested by XRD, and also the presence of nanocrystalline theta-Al2O3. 27Al MAS NMR chemical shifts, quadrupolar coupling constants and asymmetry parameters are reported for the tetrahedral and octahedral aluminium sites within theta-Al2O3.
| Item Type: | Article |
|---|---|
| Journal or Publication Title: | ChemPhysChem |
| Uncontrolled Keywords: | ball-milling, EXAFS spectroscopy, nanocrystalline oxides, sol-gel processes |
| Subjects: | UNSPECIFIED |
| Departments: | VC's Office |
| ID Code: | 52866 |
| Deposited By: | ep_importer_pure |
| Deposited On: | 29 Feb 2012 11:45 |
| Refereed?: | Yes |
| Published?: | Published |
| Last Modified: | 26 Jul 2012 20:10 |
| Identification Number: | |
| URI: | http://eprints.lancs.ac.uk/id/eprint/52866 |
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