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A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite

Laurencin, Danielle and Wong, Alan and Hanna, John V. and Dupree, Ray and Smith, Mark E. (2008) A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite. Journal of the American Chemical Society, 130 (8). pp. 2412-2413.

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Abstract

High resolution Ca-43 solid-state NMR studies of hydroxyapatite (Ca-10(PO4)(6)(OH2)) were performed at 14.1 T. The two crystallographically distinct calcium sites were unequivocally resolved by a triple-quantum magic angle spinning experiment, and the unambiguous assignment of the signals was possible using H-1-Ca-43 rotational echo double resonance and H-1-Ca-43 cross polarization magic angle spinning experiments.

Item Type: Article
Journal or Publication Title: Journal of the American Chemical Society
Subjects: UNSPECIFIED
Departments: UNSPECIFIED
ID Code: 52857
Deposited By: ep_importer_pure
Deposited On: 29 Feb 2012 09:38
Refereed?: Yes
Published?: Published
Last Modified: 23 Jul 2014 14:58
Identification Number:
URI: http://eprints.lancs.ac.uk/id/eprint/52857

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